AnalytiChem

The Importance of Accurate Analysis in the Circular Economy

In the race toward sustainable manufacturing and zero-waste operations, accurate materials analysis plays a critical role. From metals and polymers to rare earth elements and ceramics, precision in quantification, identification, and compliance enables industries to close the loop with confidence. 

Complete Traceability: Optimizing Resource Extraction with Laboratory Insights

In today’s high-stakes resource sector, whether mining for critical minerals or drilling for hydrocarbons, the margin between success and failure is increasingly defined by data quality and traceability. Laboratory analysis is no longer a post-facto box to check; it is a strategic pillar in optimizing every phase of resource extraction, from exploration to feasibility, and into production. 

Understanding the mineralogical, geochemical, and elemental composition of a sample through laboratory methods informs key decisions about whether a resource is economically extractable, how it should be processed, and whether it meets regulatory and environmental thresholds. 

241203 Sunday Creek 046

QA/QC Programs for Exploration

The foundation of any reliable resource assessment begins with a rigorous quality assurance/quality control (QA/QC) program during early exploration. 

  • Early-stage sampling and drilling campaigns must incorporate robust QA/QC protocols to avoid bias and contamination that could distort results. Laboratories support this by ensuring chain-of-custody protocols, sample preparation consistency, and statistical validation of results. 
  • Control samples, such as assay standards, blanks, and duplicates, are essential to validate your sample's assay accuracy and precision. 
  • Certified Reference Materials (CRMs) provide a benchmark for instrument and assay calibration, enabling laboratories to correct for matrix effects and instrument drift, particularly in multi-element geochemical analysis. 
  • For hydrocarbon exploration, crude oil analysis includes determining API gravity, sulfur content, and molecular fingerprinting. These lab outputs influence not only reservoir modeling but also commercial valuation. 

Ultimately, a well-structured QA/QC program instills confidence in both technical teams and financial stakeholders by ensuring the data can be trusted. 

Matching Analysis Technique to Sample Type

Not all samples are created equal—and neither are the techniques used to analyze them. The selection of analytical methodology must be aligned with the composition, expected concentration ranges, and matrix effects of the sample in question. 

XRF analysis mining industry

X-ray fluorescence (XRF) is favored for its speed and non-destructive nature, especially in hand-held, portable formats. While ideal for high-concentration elements in rocks and soils, XRF may fall short in precision for trace-level detection.

 

 

Fire Assay Circular EconomyFire assay, particularly when coupled with ICP-OES or ICP-MS finish, remains the gold standard for precious metals like gold and platinum. Its ability to extract and quantify ultra-trace levels ensures compliance with industry reporting codes. 

 

 

Inductively Coupled Plasma (ICP) techniques, ICP-OES for mid-level concentrations and ICP-MS for ultra-trace—are pivotal in characterizing critical minerals such as lithium, cobalt, and rare earth elements. These techniques offer multi-element profiling with low detection limits, which is vital in evaluating the potential of polymetallic deposits. 

To achieve maximum analytical accuracy, particularly in comparative techniques such as XRF, ICP-OES, and fire assay, it is essential to use matrix-matched standards. These are reference materials that closely replicate the chemical and physical composition of the actual sample being analyzed. Without matrix matching, factors such as inter-element interference, particle size effects, and matrix-dependent signal suppression or enhancement can lead to significant analytical bias.

By calibrating instruments and validating methods with standards that mimic the real sample matrix, laboratories can minimize systematic errors and ensure that reported concentrations truly reflect the material’s composition. This practice is especially critical when working with heterogeneous geological samples or complex ore bodies, where standard calibration curves alone are insufficient for accurate quantification. 

Ultimately, laboratory professionals must carefully consider matrix interference, detection limits, and sample preparation techniques to ensure analytical results are fit-for-purpose. 

230221-ORE-452-1

Learn more about OREAS CRMs

Read More

Using Data to Confirm Economic Viability of Extraction Projects 

High-integrity laboratory data is the foundation of technical reporting standards that govern mineral resource classification and project viability. Frameworks such as NI 43-101 (Canada), JORC (Australia), SAMREC (South Africa), and other CRIRSCO-style codes require data that is traceable, auditable, and statistically validated. These codes exist not just for compliance, but to ensure transparency, support investor confidence, and provide a reliable basis for economic decision-making. 

Laboratories contribute directly to this process by implementing rigorous QA/QC protocols, using certified reference materials, blanks, and duplicates to ensure analytical integrity. This data is then interpreted by Qualified Persons (QPs), who certify that the results meet disclosure standards. 

Accurate laboratory data is critical for defining cut-off grades, resource classifications, and reserve conversions, all of which influence financial modeling and project feasibility. In this context, laboratories are not peripheral service providers; they are central to project de-risking.

Their ability to generate consistent, high-quality, analytical data is fundamental to defining cut-off grades, estimating tonnage and grade distributions, and informing metallurgical recovery models. Ultimately, this data shapes the economic case presented to investors and regulators and determines whether a resource transitions from discovery to development. 

Ensuring Refining Process Integrity Through Laboratory Analysis

 

Refineries operate under intense conditions where precision and consistency are critical. Laboratory analysis is a cornerstone in maintaining process integrity, enabling continuous optimization, compliance, and efficiency. Through advanced testing methodologies, refineries can identify process inefficiencies, minimize product variability, and meet the stringent demands of global fuel markets. 

Generating trusted data to drive process optimization

Laboratory services empower refineries to make data-driven decisions by providing accurate and repeatable results across a range of critical parameters. In fuel analysis, whether you are analyzing viscosity, sulfur content via XRF, or hydrocarbon profiles using gas chromatography (GC), trusted data supports operational excellence. 

Utilizing certified reference materials, especially when performing comparative techniques, and adhering to ASTM and ISO methods ensures consistent quality control. This analytical backbone enables proactive adjustments in real-time, helping to reduce waste, optimize yields, and extend equipment lifespan in demanding environments. 

GOLD Crms

Read about Homogeneity in CRMs

Learn More

Meeting Industry Standards

Meeting industry standards during the refining of minerals or petroleum products is essential to ensure product quality, operational safety, and regulatory compliance. Throughout these refining processes, adherence to established methodologies, such as those defined by ASTM, ISO, and other international bodies, helps maintain consistency and reliability in results. For petroleum refining, standards like ASTM D2622 are used to monitor critical parameters such as sulfur content.

In mineral beneficiation, precise testing ensures that valuable elements are efficiently separated and processed, often under strict environmental and export regulations. Laboratory analysis also supports batch certification, equipment calibration, and process optimization, reducing variability and waste. Ultimately, aligning with industry standards strengthens quality assurance, builds stakeholder trust, and enables seamless integration into global supply chains. 

Compliance with Global Regulatory Requirements

Laboratory testing plays a crucial role in ensuring compliance with global regulatory requirements that govern fuel composition, emissions, and environmental impact. Regulations such as EPA Tier III in the United States mandate significant reductions in sulfur content and other pollutants in gasoline and diesel fuels, aimed at cutting vehicle emissions and improving air quality.

Similarly, the Directive (EU) 2016/802 regulates the sulfur content of certain liquid fuels across the European Union, requiring rigorous analytical validation to ensure that limits are not exceeded. To meet these strict standards, refineries and fuel producers rely on precise lab testing methods to generate traceable, reproducible data. This ensures that products not only meet legal thresholds but are also aligned with international trade requirements and environmental sustainability goals.

Product Highlight

Check out our range of products to help you optimize resource extraction

CONOSTAN® Sulfur Standards

AC_SINMonitoring sulfur content is a critical part of maintaining refining efficiency and meeting global fuel specifications. CONOSTAN Sulfur Standards are: 

  • Ready-to-use solutions ranging from ultra-low levels (0.5 ppm) to high-concentration blends up to 60,000 ppm, ensuring accurate calibration across the full analytical range.  
  • Available in matrices such as Mineral Oil, Diesel, Residual Oil, Isooctane, Biodiesel, Xylene, Ethanol, Crude Oil and PremiSolv 
  • Aligned with major ASTM and ISO methods, supporting regulatory compliance and traceable reporting.  
  • For labs facing unique sample challenges, custom concentrations and matrix formulations can be produced following technical approval—delivering confidence in every measurement. 
 Learn more CONOSTAN Sulfur in Oil Standards 

XRF Cups & Film

XRF_film_cells_collage_NoSCPIn XRF analysis, controlling contamination and preserving instrument integrity is essential for maintaining repeatable, defensible data in refinery environments.  

Disposable XRF sample cups—available in single- or double-open-ended formats and compatible with most standard holders—provide clean, consistent sample presentation for both liquids and powders. 

Thin films, offered as Easy-Snap sheets, pre-cut circles, or continuous rolls, support a wide range of application needs with thicknesses from 2.5 μm to 12 μm. With various materials available, including Mylar,® polypropylene and Etnom,® labs can select optimal film chemistries to minimize background interference and protect instrument components throughout continuous process monitoring.   

Learn more XRF cells and thin film

Graphite Crucibles

cruciblesHigh-purity graphite crucibles play a central role in fusion-based sample preparation, helping laboratories generate precise analytical results even for complex refining matrices.

Their thermal stability, low impurity profile, and consistent performance support high-temperature workflows such as metals fusion, loss-on-ignition studies, and elemental determinations essential for process validation.

By ensuring clean, reliable digestion or fusion conditions, these crucibles contribute directly to the integrity of downstream XRF and ICP measurements—strengthening the analytical foundation refineries depend on for quality control and regulatory alignment. 

ICP Standards

products-icp-standardsFor ICP-OES workflows used to verify elemental composition in fuels, feedstocks, catalysts, and process streams, high-quality calibration standards are essential to achieving accurate, reproducible results. 

AnalytiChem provides a broad range of single-element solutions alongside multi-element blends tailored to refinery-specific applications.  

When unique composition requirements arise, custom formulations can be developed following a technical feasibility review—ensuring matrix-matched accuracy for even the most challenging samples.  

These standards uphold method precision and support compliance with global industry methods, reinforcing the analytical confidence required for process optimization. 

Request a Custom ICP Standard from AnalytiChem

Advanced Materials Backed by Analytical Excellence 

As industries move toward cleaner, more efficient technologies, the materials they rely on must be validated with high confidence. From next-gen batteries to sustainable building materials, laboratory analysis underpins the development and scale-up of advanced materials. 

Material Analysis Powering Innovation 

Innovation in fields like battery manufacturing and green cement requires rigorous material characterization. Analytical techniques assess performance-critical features such as elemental composition, phase distribution, and thermal stability—ensuring materials meet both design expectations and regulatory standards. 

By applying precise laboratory analysis during R&D and production, manufacturers gain the confidence to innovate while maintaining consistent quality. 

Closing the Loop with Data-Driven Recycling

Circular economy data driven recycling

In a circular economy, the ability to reclaim and reuse valuable materials depends heavily on data. Laboratory analysis plays a critical role in transforming waste into valuable feedstock, improving process efficiencies, and validating the purity and usability of recycled materials. 

Integrating Analysis with Recycling

Recycling processes, particularly for EV batteries, Li-NMC cathodes, and automotive catalysts, demand high-precision testing. Techniques like handheld XRF enable on-the-spot material identification, supporting fast and reliable sorting. 

Laboratory data ensures recycled materials are suitable for reintegration into manufacturing streams, closing the loop and minimizing reliance on virgin resources.  

Sample Preparation for Complex Matrices

Accurate analysis starts with proper sample preparation. Recyclers often deal with diverse and complex matrices that require specialized methods such as acid digestion, microwave digestion, or digestion blocks to break down samples for elemental analysis. Investing in reliable sample preparation ensures downstream accuracy and actionable data. 

Extending Lifecycles Through Insight: 
How In-Service Testing Keeps Assets in Use, Longer

Prevent costly failures with predictive and preventative maintenance strategies. In-service oil testing, RDE spectroscopy, and wear metals analysis (e.g., using Conostan standards) help identify early signs of equipment degradation, allowing timely interventions and maximizing asset lifespan.

Product Highlight

Check out our range of products to help you reclaim and reuse valuable materials

Critical Material Recycling

critical_materialAnalytiChem’s Critical Material Recycling CRMs are matrix-matched to some of the industry’s hardest-to-source materials, including spent automotive catalysts for platinum (Pt, palladium (Pd) and rhodium (Rh), and also containing rare earth elements.

With full 100% composition transparency on every certificate of analysis, these CRMs provide the analytical confidence required to validate recovery efficiency and certify recycled material quality.  

By supporting precise, traceable measurements, they help recyclers maximize the value of materials well beyond their first use-life. 

Black Mass

ac_BlackMass_bottle-1As EV battery recycling accelerates, reliable characterization of black mass is critical for ensuring high-value recovery of lithium, nickel, manganese, and cobalt. 

AnalytiChem’s Black Mass CRM is sourced directly from real NMC battery waste, delivering true-to-life matrix matching that labs can trust. 

This authenticity minimizes analytical bias and strengthens confidence in yield calculations, purity verification, and downstream processing decisions. By anchoring analysis to accurate reference materials, recyclers gain the data needed to reintroduce recovered metals back into production cycles—closing the loop on critical battery materials. 

SNRG Block™

SNRG Block 1000x1000Effective recycling depends on breaking down heterogeneous, complex matrices into analyzable solutions.  

The SNRG Block offers a streamlined hot-block digestion platform designed to deliver consistent, reliable sample breakdown for metals, catalysts, and battery waste.  

By ensuring controlled heating and uniform digestion, the SNRG Block helps laboratories generate cleaner extracts, reduce prep variability, and improve measurement accuracy across techniques like ICP-OES and ICP-MS.  

This dependable preparation step strengthens the integrity of every recycling dataset—supporting more informed recovery, sorting, and process optimization decisions.

High Purity Acids

AnalytiChem High Purity AcidsTrace-level accuracy is only possible when every step of the workflow is free from contamination.  AnalytiChem’s high purity acids are engineered specifically for sample preparation in demanding recycling environments, ensuring no background contamination is introduced during digestion or dilution.  

Their exceptional purity supports ultra-low detection limits in ICP and other elemental analysis methods, enabling recyclers to quantify valuable metals with confidence.

By protecting analytical integrity at the earliest stages of preparation, high purity acids play a critical role in validating reclaimed material quality and driving closed-loop material recovery. 

We're here to answer your questions

You May Also Like